Organic Chemistry Lab

 

If the solubility of cholesterol in methanol were 1 g/96 mL at 20ºC and 1 g/4.1 mL at 80ºC, what is the absolute minimum amount of methanol needed to recrystallize 5.13 g cholesterol? Report the number of mL to the nearest whole number.
In recrystallization experiments, not all of the starting material is ever recovered, even if the initial material was 100% pure. To determine the % recovery, the ratio of final to starting masses of material is taken and converted into a percentage. In an experiment, 5.7 g of impure fluorene is recrystallized in 10 ml ethanol. After filtration and drying, 5.5 g of fluorene crystals are found on the filter paper. What is the percent recovery? List the percent to the nearest whole number and do not include the % sign.
If the solubility of cholesterol in methanol were 1 g/99 mL at 20ºC and 1 g/4.2 mL at 80ºC, what is the maximum mass of cholesterol that could be recrystallized from 5.44 g cholesterol? Report the number of grams to two decimal places.
Calculate the maximum % recovery possible if the solubility at room temperature is 1g/461 mL and at the boiling temperature of the solvent is 1g/14 mL. Report your answer as a percentage to the nearest whole number, without the percent sign.
It is important to always minimize the amount of solvent used, allowing for evaporation. If we add a relatively large excess, we expect our recrystallization to produce lower percent recoveries. A common mistake is to misplace the decimal, resulting in addition of 11x the solvent instead of the recommended 1.1x. If a substance dissolves in a solvent at 1g/459 mL at room temperature and at 1g/13 mL at the solvent’s boiling point, what would be the maximum expected amount recovered if using 11x the minimum amount of solvent in recrystallizing 10 g of the substance? Report your answer in grams to one decimal place.

Sample Solution

The development approach is what I talked about at the beginning of the paper. I am going over this theory repeatedly because this is what I believe makes these monsters and I think it can be stopped. This approach goes into more depth about the childhood symptoms. This approach talks about the childhood behavior of bed-wetting, arson and torturing of animals. The bed-wetting is said to be a form of sadistic and hostile rebellion towards parents. Fire setting is associated with violence and torturing animals is a further form of rebellion against keeping pets as cherished friends (Mukherjee, 1998). Physical abuse as a child also plays a prominent role in the development of a serial killer. This abuse creates mistrust, an inability to establish meaningful personal or sexual relationships, feelings of low self-worth, lack of social skills, a sense of helplessness, inability to make decisions, and inability to plan life goals. The sexual abuse will make a person withdrawal into a fantasy life. To protect themselves from going crazy, the people being abused may pretend that the abuse is actually happening to someone else. After a person is abused so long, their fantasy world becomes reality and the killings could start.

The personality approach to serial killing is a broad topic that holds many controversies. Aside from psychopathic personality disorder, other personality traits have been identified as contributing to serial killer behavior. Traits of impulsiveness, low empathy and poor social skills have been found in serial killers. Others traits such as antisocial behavior, and hypersensitivity to criticism come from the serial killers with low self-esteem (Horse, 2001, 2). If intelligence can be associated as a personality variable, then average to high intelligence is likely to assist a serial killer in avoiding police detection and capture. This might explain why such levels of intelligence are found in serial murderers and it takes so long for law enforcement to finally track these killers down (Mukherjee, 1998, 7). The role of personality in the study of serial killers is an area of continuous debate. The proper testi

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